[AMMRL] Pseudo 2D for 31P kinetics

From: Thusitha Jayasundera via groups.io <thusitha.jayasundera=bc.edu_at_groups.io>
Date: Thu, 02 Apr 2026 11:22:54 -0700

Hello all--I have been trying to get a pseudo 2D experiment for a 31P kinetics
experiment to work on automation (the 1D variant works great, thanks to the
guidance of Eric Johnson from Bruker). After lots of help from several additional
patient experts, I was able to make some progress--but run into an error when
I include the ZGOPTIONS as instructed i.e. the line -DCALC_SP -DCALC_SPOFFS
for ZGOPTIONS (to define the bandwidth and position of the selective pulse
with CNST55 and CNST21) results in an error. The system is a 500 MHz Bruker
NEO with a Prodigy probe...

If I manually load the saved parameter set, I am able to run the experiment
with no errors; the attached pulse sequence is displayed on Topspin. If I
add the ZGOPTIONS, the two attached error messages appear (one in the
acquisition window, the other when attempting to visualize the pulse
sequence--which I also have attached here).

I am assuming that I'm making a very simple and embarrassing mistake, and
therefore would appreciate any available advice!

With many thanks in advance,

TJ.


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Received on Thu Apr 02 2026 - 11:23:27 MST

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