MAGIC ANGLE CALIBRATION

From: Lab. Resonancia Magnetica Nuclear <agrmn_at_xanum.uam.mx>
Date: Fri, 26 Sep 2003 17:02:17 -0500

Dear ammrl members,

We have just instaled a new 7mm, 17O-39K MAS probe in our Bruker
ASX300.

As we do not know if the magic angle is correcty set, we alrready tried
several substances looking for a chemichal shift anisotropy similiar to
the one found in 79Br, in KBr, that allow us to do this assesment.
Unfortunately we have not have any success.

I hope that some of you would have experience working with these
frequencies, and let us know, what substance will be the best suited for
this purpose. I would do realy apprecite your help.

Thanks in advance.

Atilano Gutierrez
NMR Lab
Universidad Autónoma Metropolitana
Unidad Iztapalapa
Mexico, city
e-mail: agrmn_at_xanum.uam.mx
           agu44_at_hotmail.com
Phone: (525) 5558046541
Received on Fri Sep 26 2003 - 15:16:33 MST

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