Dear spinlanders,
I need to measure quantitative HSQCs and have been searching and writing
to authors of some of the papers I read to inquire for a pulse program
and/or dataset, sadly to no avail. So again I thought of tapping into
the beehive knowledge here, to ask whether anyone has implemented one
(ideally HSQC0, qqHSQC or qaHSQC on a Bruker machine and even more
ideally with an example dataset). Should any publication result (which I
surely hope), a place in the acknowledgements is reserved for you of
course. Any hands-on insights into which of the three mentionedpulse
programs worked best in your hands will be appreciated as well. I will
summarize the results for all if there are any, of course omitting the
actual datasets and stuff.
Thank you in advance and all the best, André
PS: A summary of my last request on an MASII error (from March!!!!) is
still pending because I (or actually the Spin-Doc) still have not found
the cause but was able to fix the problem with the help of a replacement
from the Spin-Doc, thank for that!
--
Dr. André Dallmann
Leiter der NMR-Abteilung
Email: andre.dallmann_at_chemie.hu-berlin.de
Raum: 0'103
Telefon: 7341
Handy: 01797657855
ORCID-ID: https://orcid.org/0000-0002-0141-2635
Webseite: https://www.chemie.hu-berlin.de/en/forschung-en/nmr-spectroscopy/nmr-spectroscopy?set_language=en
Adresse:
Humboldt Universität zu Berlin
Institut für Chemie
AG NMR
Brook-Taylor-Str. 2
12489 Berlin
Deutschland
Received on Tue Oct 25 2022 - 19:08:32 MST