Re: Locking on the standard
Juergen Schulte (schulte@binghamton.edu)
Tue, 12 May 1998 14:10:45 -0400 (EDT)
Besides using unique shim matrix files and H-1 or C-13 job parameter files
for different solvents to allow the students the easiest start possible I
found it to be the simplest solution to have every student, after he/she
has finished his/her spectrometer session, execute a little EXE program
("EXE FINISH"), which I wrote for our Bruker AM and ACs.
It resets the spectrometer to a predefined condition:
- set spinning speed and turn on sample spinning
- turn off decoupler
- load proton parameters
- load shim file for the standard sample
- set the Bo shim and lock the sample
- start auto shim procedure
- display a message about our user policies
and other neat (probably useless) stuff
The whole procedure is started with one command and the spectrometer will
be available for the next user after 1-2 minutes.
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Juergen Schulte ! !
NMR Specialist U
Department of Chemistry ~
SUNY Binghamton Phone: (607) 777-4405
Binghamton, NY 13902-6016 Fax: (607) 777-4478
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schulte@binghamton.edu schulte@chemiris.chem.binghamton.edu
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