Hello to all,
Thank you so much to everyone who responded, your help was invaluable.
I wanted to share with everyone the information I received:
"A study of polyhydroxyalkanoates by quantitative 31P NMR Spectroscopy:
Molecular weight and chain cleavage".
A. Spyros, D. S. Argyropoulos, and R. H. Marchessault, Macromolecules 1997,
30, 327.
"Quantitative determination of the distribution of free hydroxylic and
carboxylic groups in unsaturated polyester and alkyd resins by 31P NMR
spectroscopy".
A. Spyros, J. Appl. Polym. Sci., 2002, 83, 1635.
"An Enantioselective Synthesis of (S)-(+)-3-Aminomethyl-5-methylhexanoic
Acid via Asymmetric Hydrogenation"
Mark J. Burk, Pieter D. de Koning, Todd M. Grote, Marvin S. Hoekstra,
Garrett Hoge, Rex A. Jennings, William S. Kissel, Tung V. Le, Ian C. Lennon,
Thomas A. Mulhern, James A. Ramsden, and Robert A. Wade, J. Org. Chem.;
2003; 68(14) pp 5731 - 5734
"Spectroscopic Characterization of the Degradation Products of P-Containing
Polymer Additives". Brandolini, Garcia, and Truitt, Spectroscopy, 7(3),
p.34-39 (1992)
Do a literature search on "Peter Rinaldi"; he works with polymers and has
used 31P NMR based methods.
Take a look at Matthew Espe at the University of Akron.
Todd Alam's research at Sandia National Labs - he has published papers on
31P NMR and also does polymer characterization.
Do a literature search on polyphosphazanes.
Again, thank you to everyone for your help.
Adrienne B. Hoeglund
NMR Specialist
AOC, LLC.
Received on Thu May 27 2004 - 12:49:16 MST