Hi Greg
as you can see from previous responses this is not a straight forward issue.
In addition to the methods mentioned before there is also the option to run
the second part of an acquisition as a pseudo NUS experiment. The NUS schedule
would include all the missing FID's in their normal order. The scrip= t from
Youlin could then merge the two parts.
I am more worried about reaching a sufficiently "identical state" of the
cryoprobe after a termal cycle. If the probe does not land at the exact same
termperature you might see subtle changes in for example the signal phase.
A fraction of a degree difference would still be noticeable in the data.
Clemens
On 7/10/2023 6:44 AM, Heffron, Gregory J. wrote:
Hi All,
I write to ask the group if anyone knows how best to stop an acquisition in
progress on Bruker NEO systems. We are somewhat familiar with commands to
do this, but have not had much success in getting them to work. Specifically,
we would like to be able to stop an acquisition in progress, then start it at
a later time from the point it was stopped, OR be able to stop an acquisition,
then restart it by calculating appropriate delays and add the data together
when the total experiment is finished. We ask about this because we suffer
occasionally from interruptions to experiments with cryoprobes due to cooling
water issues.
Any ideas are greatly appreciated, and we will post a summary.
Best,
Greg
Gregory J. Heffron | Director, Biomolecular NMR Facility | Visiting Scientist, Dana-Farber Cancer Institute | Department of Cancer Biology
Harvard Medical School 240 Longwood Ave. | Boston, MA 02115 | Fax :617-432-4383
--
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====================
Clemens Anklin Ph.D. Vice President
Bruker BioSpin NMR Applications & Training
15 Fortune Drive NEW Phone: 978-313-5NMR(5667)
Billerica MA 01821 twitter: _at_canklin
http://www.bruker.com
e-mail: clemens.anklin_at_bruker.com
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Received on Mon Jul 10 2023 - 15:09:46 MST