Dear Spinlanders,
I am interested in doing LC-NMR on a limited budget, so I do not have a
flow probe. I got a flowcell from Wilmad designed after that used for
stopped flow measurements [Appl. Spectr. 1997, 41(5), 847-851]. I was
wondering if anyone out there has had experience with this type of setup
on a Bruker system. We have an Avance 400 running Topspin 1.3. What I
was hoping to do was to run time slice experiments rather than on-flow
measurements, but if on-flow could be accomplished with some measure of
sensitivity, that would be great as well. What I had in mind was
collecting a set of arrayed experiments in automation if possible. If
anyone has experience with this, I would greatly appreciate any advice
on this topic.
Best,
Rick
Richard W. Fitch
Department of Chemistry
Indiana State University
600 Chestnut Street
Science Building, Rm. S35E
Terre Haute, IN 47809
Phone: (812) 237-2244
Fax: (812) 237-2232
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Received on Wed Jul 05 2006 - 13:30:58 MST