Re: Mini Survey....

Feng Qiu (fqiu@bmb-fs1.biochem.okstate.edu)
Tue, 24 Sep 1996 16:00:48 -0500

Hello, Dr. Shoemaker,
I would like to see your summary.
I believe you need two full band or high band channel to do the first
experiment, Broad band cannot go to 19F or 1H, sure you need 19F and 1H
two channel probe too.
Second experiment, you may just do two experiment: one dec 1H, observe
13C, second: dec 19F, observe 13C, you will have all information you
want, and you can just do it on regular Four nuclei probe (1H, 19F; 13C,
31P).
Feng

Richard K. Shoemaker wrote:
>
> Dear NMR Managers,
>
> This inquiry is primarily for university Chemistry dept. facilities.
>
> Our instrumentation is aging wrt/ modern instrumentation, and I was
> wondering how many of you have instruments in your facility which can
> routinely do one of both of the following:
>
> 1) 19F-1H double resonance (HETCOR/COSY).
>
> 2) 19F-1H (simultaneously) decoupled C-13 NMR.
>
> I have a user who _really_ needs the above capability. #1 would simply
> require an H-F dual probe. Assuming that my Omega-500 could use the observe
> channel for one freq. and I could use the BB-decoupler to pulse the other
> freq. I'm 90% sure that it would work on my Omega-500 (BB on both channels),
> but I would appreciate hearing from any Omega owners who are doing H-F
> double resonance experiments.
>
> I would need a third channel to do #2 above, which would mean a complete
> console upgrade (unless anyone has the hardware to add the 3rd channel to
> my 293-based Omega-500 that they want to sell me 8-).
>
> PLEASE E-Mail me your responses, and indicate whether you would mind having
> your facility listed in a summary to be posted later.
>
> Thanks to all for your responses...I need this information rather quickly.
>
> Best Regards,
>
> Rich Shoemaker
> --
> Richard Shoemaker, Ph.D. Phone--(402) 472-6255
> Instrumentation Director, Chemistry FAX---- -6964
> Research Associate Professor, Chemistry
> University of Nebraska-Lincoln
> URL: http://wwitch.unl.edu/nmrlab.html

-- 
Feng Qiu, Ph.D.
NMR Facility Manager
Department of Chemistry       Phone: (405)744-4308
Oklahoma State University     Fax:   (405)744-6007
Stillwater, OK 74078          E-mail: fqiu@bmb-fs1.biochem.okstate.edu