AMMRL: Bruker HSQC-DOSY

From: Philip Dennison <dennison_at_uci.edu>
Date: Fri, 18 Sep 2015 15:43:12 -0700

Hi all,

I've been struggling to get good signals from the 3D Bruker HSQC DOSY
experiment "idosyhsqc3d". This is for 1H-15N correlation, and the
standard 2D HSQC gives very clean spectra.

I am using TopSpin 3.1 on an AVANCE600 with a TBI probe.

There are some obscure parameter settings, like the KAPPA "unbalancing
factor" which have me baffled.

Has anyone else used this experiment?

Thanks,

Phil.

-- 
Dr Phil Dennison
NMR Facility Director           (949)824-6010 (office)
Department of Chemistry         (949)824-5649 (lab)
University of California        (949)824-8571 (fax)
Irvine, CA 92697-2025           dennison_at_uci.edu
USA

Received on Fri Sep 18 2015 - 12:43:15 MST