Hi all,
I am trying to set up an H1-Si29 gHMBC and not having much luck. Using TMS in CDCl3 with coupling constant setting of 7 Hz. I assume the issue is with the gradient settings but I haven't been able to fix it. Any advice, or if anyone has a set of parameters they could forward (vnmrj or topspin), would be appreciated.
Thanks,
David Richardson, Ph.D.
NMR Instrumentation Specialist
University of Central Florida
Department of Chemistry
PO Box 162366
Orlando, FL 32816-2366
david.richardson_at_ucf.edu<mailto:david.richardson_at_ucf.edu>
office: PS236 (407) 823-2961<tel:%28407%29%20823-2961>
lab: CH335 (407) 882-0117<tel:%28407%29%20882-0117>, PS151 (407) 823-2906<tel:%28407%29%20823-2906>
fax: (407) 823-2252<tel:%28407%29%20823-2252>
Received on Mon Sep 19 2011 - 03:48:48 MST