Re: solid state nmr education

Joseph (vaughn@pro.sb.fsu.edu)
Tue, 12 Oct 1999 15:58:21 -0400

Colleagues
Thanks for all of the responses! For those of you who requested it, here
is the list of references I got.

"150 and More Basic NMR EXperiments" by Braun,
Kalinowski and Berger

The latest edition includes solid state experiments.

>1. R.E. Richards, "NMR Spectra of Organic Solids," in "Determination
>of Organic Structures by Physical Methods, Vol. 2, F.C. Nachod and
>W.D. Phillips, Eds., Academic Press, NY, 1962, Ch. 8.
>
>2. J. Jenner, "Thermodynamics of Spin Systems in Solids," Adv. Magn.
>Reson., 3, 205 (1968).
>
>3. P.S. Allen, "NMR Studies of Molecular Motion in Solids," MTP Int.
>Rev. Sci., Phys. Chem., Ser. 1, 4, 43 (1972).
>
>4. E.R. Andrew, "The Narrowing of NMR Spectra of Solids by High-Speed
>Specimen Rotation and the Resolution of Chemical Shift and Spin
>Multiplet Structures for Solids," Prog. Nucl. Magn. Reson. Spectrosc.,
>8, 1 (1972).
>
>5. P. Mansfield, "Pulsed NMR in Solids," Prog. Nucl. Magn. Reson.
>Spectrosc., 8, 41 (1972).
>
>6. H. Pfeifer, "NMR and Relaxation of Molecules Adsorbed on Solids,"
>NMR Basic Prin. Prog., 7, 53 (1972).
>
>7. A. Weiss, "NMR in Solid-State Chemistry," Angew. Chem., Int. Ed.
>Engl., 11, 607 (1972).
>
>8. E.R. Andrew, "High-Resolution NMR in Solids," MTP Int. Rev. Sci.,
>Phys. Chem., Ser. 2, 4, 173 (1975).
>
>9. J. Ebert and G. Seifert, "NMR in Solids," Hilger, London, 1975.
>
>10. P.C. Taylor, J.F. Baugher, and H.M. Kriz, "Magnetic Resonance
>Spectra in Polycrystalline Solids," Chem. Rev., 75, 203 (1975).
>
>11. U. Haeberlen, "High Resolution NMR in Solids: Selective
>Averaging," Academic Press, NY, 1976 (Supplement No. 1 to Adv. Magn.
>Reson.).
>
>12. L. Van Gerven, Ed., "NMR in Solids," Plenum Press, NY, NATO
>Advanced Study Institute Series, Series B, 22 (1977).
>
>13. R.W. Vaughan, "High Resolution Solid State NMR," Annu. Rev. Phys.
>Chem., 29, 397 (1978).
>
>14. G.R. Hays, "High Resolution 13C Solid State NMR Spectroscopy,"
>Analyst (London), 107, 241 (1982).
>
>15. J.R. Layerla, C.S. Yannoni, and C.A. Fyfe, "Chemical Applications
>of Variable Temperature CP/MASS NMR Spectroscopy in Solids," Acc.
>Chem. Res., 15, 208 (1982).
>
>16. F.P. Miknis, "NMR Studies of Solid Fossil Fuels," Magn. Reson.
>Rev., 7, 87 (1982).
>
>17. S.J. Opella, "Solid State NMR of Biological Systems," Annu. Rev.
>Phys. Chem., 33, 533 (1982).
>
>18. F.A. Rushworth, "Wide-Line NMR and Relaxation Processes in Ionic
>and Molecular Solids," Magn. Reson. Rev., 7, 197 (1982).
>
>19. R.E. Wasylishen and C.A. Fyfe, "High-Resolution NMR of Solids,"
>Annu. Rep. NMR Spectrosc., 12, 1 (1982).
>
>20. C.S. Yannoni, "High-Resolution NMR in Solids: The CPMAS
>Experiment," Acc. Chem. Res., 15, 201 (1982).
>
>21. B.C. Gerstein, "High-Resolution NMR Spectrometry of Solids," Anal.
>Chem., 55 (1983). Part 1, 718A; Part 2, 899A.
>
>22. C.A. Fyfe, "Solid State NMR for Chemists," CFC Press, Guelph,
>Ontario, 1983.
>
>23. C.A. Fyfe, J.M. Thomas, J. Klinowski, G.C. Gobbi, S. Ramadas, and
>M.W. Anderson, "MASS-NMR Spectroscopy and the Structure of Zeolites,"
>Angew. Chem., Int. Ed. Engl., 22, 259 (1983).
>
>24. R.K. Harris, "High Resolution Solid-State NMR Studies of Group IV
>Elements," in "The Multinuclear Approach to NMR Spectroscopy," J.B.
>Lambert and F.G. Riddell, Eds., Reidel, Hingham, MA, NATO Advanced
>Study Institute Series, Series C, 103, 361 (1983).
>
>25. M. Mehring, "Principles of High Resolution NMR in Solids," 2nd
>ed., Springer-Verlag, Berlin, 1983.
>
>26. K.J. Packer, "NMR in Solids," in "The Multinuclear Approach to NMR
>Spectroscopy," J.B. Lambert and F.G. Riddell, Eds., Reidel, Hingham,
>MA, NATO Advanced Study Institute Series, Series C, 103, 111 (1983).
>
>27. B.C. Gerstein, "High-Resolution Solid-State NMR of 13C," Top. C-13
>NMR Spectrosc., 4, 123 (1984).
>
>28. J. Klinowski, "NMR Studies of Zeolites," Prog. Nucl. Magn. Reson.
>Spectrosc., 16, 237 (1984).
>
>29. G.E. Maciel, "High-Resolution NMR of Solids," Science (Washington,
>DC), 226, 282 (1984).
>
>30. D.E. Axelson, "Solid State NMR of Fossil Fuels: An Experimental
>Approach," Multiscience Publications, Montreal, Canada, 1985.
>
>31. P.J. Bray, "NMR Studies of Glass Structure," J. Non-Cryst. Solids,
>73, 19 (1985).
>
>32. A.D.H. Clague, "High Resolution Solid State NMR: Theory and
>Applications," Catalysis, 7, 75 (1985).
>
>33. C. Dybowski, "Solid State Investigations via NMR," CHEMTECH, 15,
>186 (1985).
>
>34. B.C. Gerstein and C.R. Dybowski, "Transient Techniques in NMR of
>Solids: An Introduction to Theory and Practice," Academic Press,
>Orlando, FL, 1985.
>
>35. U. Haeberlen, "Multiple Pulse Techniques in Solid State NMR,"
>Magn. Reson. Rev., 10, 81 (1985).
>
>36. R.A. Kinsey, R.J. Kirkpatrick, J. Hower, K.A. Smith, and E.
>Oldfield, "High Resolution Al-27 and Si-29 NMR Spectroscopic Study of
>Layer Silicates, Including Clay Minerals," Am. Mineral., 70, 537
>(1985).
>
>37. R.J. Kirkpatrick, K.A. Smith, S. Schramm, G. Turner, and W.H.
>Yang, "Solid-State NMR Spectroscopy of Minerals," Annu. Rev. Earth
>Planet. Sci., 13, 29 (1985).
>
>38. E. Oldfield and R.J. Kirkpatrick, "High-Resolution NMR of
>Inorganic Solids," Science (Washington, DC), 227, 1537 (1985).
>
>39. E. Oldfield, H.K.C. Timken, B. Montez, and R. Ramachandran,
>"High-Resolution Solid State NMR of Quadrupolar Nuclei," Nature
>(London), 318, 163 (1985).
>
>40. S.J. Opella and L.M. Gierasch, "Solid State NMR of Peptides,"
>Peptides, 7, 405 (1985).
>
>41. J.M. Thomas and J. Klinowski, "The Study of Aluminosilicate and
>Related Catalysts by High Resolution Solid-State NMR Spectroscopy,"
>Adv. Catalysis, 33, 199 (1985).
>
>42. G.A. Webb, "NMR Spectroscopy," Annu. Rep. Prog. Chem., Sect. C,
>82, 3 (1985).
>
>43. R.A. Wind, M.J. Duijvestign, C. Van Der Lugt, A. Manenschijn, and
>J. Vriend, "Applications of Dynamic Nuclear Polarization in 13C NMR in
>Solids," Prog. Nucl. Magn. Reson. Spectrosc., 17, 33 (1985).
>
>44. P.J. Bray and M.L. Lui, "NMR Study of Structure and Bonding in
>Glasses," in "Structure and Bonding in Noncrystalline Solids," G.E.
>Walrafen and A.G. Revesz, Eds., Plenum Press, NY, 1986, p. 285.
>
>45. L. Jelinski, "NMR of Plastics," CHEMTECH, 16, 186 (1986).
>
>46. R.J. Kirkpatrick, T. Dunn, S. Schramm, K.A. Smith, R. Oestrike,
>and G. Turner, "Magic-Angle Sample-Spinning NMR Spectroscopy of
>Silicate Glasses: a Review," in "Structure and Bonding in
>Noncrystalline Solids," G.E. Walrafen and A.G. Revesz, Eds., Plenum
>Press, NY, 1986, p. 303.
>
>47. J. Klinowski and J.M. Thomas, "The Magic Angle and All That:
>Probing the Structure of Solids Using NMR," Endeavour, 10, 2 (1986).
>
>48. H. Saito, "Conformation-dependent 13C Chemical Shifts: A New Means
>of Characterization as Obtained by High-Resolution Solid-State 13C
>NMR," Magn. Reson. Chem., 24, 835 (1986).
>
>49. C.P. Slichter, "Probing Phenomena at Metal Surfaces by NMR," Annu.
>Rev. Phys. Chem., 37, 25 (1986).
>
>50. T. Terao and F. Imashiro, "Stereochemical Studies in the Solid
>State," in "Applications of NMR Spectroscopy to Problems in
>Stereochemistry and Conformational Analysis," Y. Takeuchi and A.P.
>Marchand, Eds., VCH Publishers, Deerfield Beach, FL, 1986, Ch. 4
>
>51. L.W. Jelinski and M.T. Melchior, "High-Resolution NMR of Solids,"
>in "NMR Spectroscopy Techniques," C. Dybowski and R.L. Lichter, Eds.,
>Marcel Dekker, NY, 1987, Ch. 6.
>
>52. M.A. Wilson, "NMR Techniques and Applications in Geochemistry and
>Soil Chemistry," Pergamon Press, NY, 1987.
>
>53. S. Aime, "Effects of Molecular Motions on NMR Parameters of Solid
>State Spectra," in "Time Domain in Surface and Structural Dynamics,"
>G.J. Long and F. Grandjean, Eds., Reidel, Hingham, MA, NATO Advanced
>Study Institute Series, Series C, 228 , 65 (1988).
>
>54. E.R. Andrew, "Time Domain NMR and Magic Angle Spinning," in "Time
>Domain in Surface and Structural Dynamics," G.J. Long and F.
>Grandjean, Eds., Reidel, Hingham, MA, NATO Advanced Study Institute
>Series, Series C, 228 , 31 (1988).
>
>55. B. Bl=FCmich and H.W. Spiess, "Two-Dimensional Solid-State NMR
>Spectroscopy: New Possibilities for the Investigation of the Structure
>and Dynamics of Solid Polymers," Angew. Chem., Int. Ed. Engl., 27,
>1655 (1988).
>
>56. N.J. Clayden, "Chemical, Molecular and Spin Dynamics," in "Time
>Domain in Surface and Structural Dynamics," G.J. Long and F.
>Grandjean, Eds., Reidel, Hingham, MA, NATO Advanced Study Institute
>Series, Series C, 228 , 49 (1988).
>
>57. N.J. Clayden, "Solid State NMR Spectroscopy in Inorganic
>Chemistry," Chem. Scr., 28, 211 (1988).
>
>58. G. Englehardt and D. Michel, "High-Resolution Solid-State NMR of
>Silicates and Zeolites," Wiley, NY, 1988.
>
>59. J.F. Haw, "Variable-Temperature Solid-State NMR Spectroscopy,"
>Anal. Chem., 60, 559A (1988).
>
>60. R.J. Kirkpatrick, "MAS NMR Spectroscopy of Minearls and Glasses,"
>in "Spectroscopic Methods in Mineralogy and Geology," F.C. Hawthorne,
>Ed., Mineralogical Society of America, Washington, DC, 1988, p. 341.
>
>61. J. Klinowski, "Recent Advances in Solid State NMR of Zeolites,"
>Annu. Rev. Mater. Sci., 18, 189 (1988).
>
>62. S.O. Smith and R.G. Griffin, "High-Resolution Solid-State NMR of
>Proteins," Annu. Rev. Phys. Chem., 39, 511 (1988).
>
>63. R. Voelkel, "High-Resolution Solid-State 13C-NMR Spectroscopy of
>Polymers," Angew. Chem., Int. Ed. Engl., 27, 1468 (1988).
>
>64. R.L. Armstrong, "Displacive Order-Disorder Crossover in Perovskite
>and Antifluorite Crystals Undergoing Rotational Phase Transitions,"
>Prog. Nucl. Magn. Reson. Spectrosc., 21, 151 (1989).
>
>65. B.F. Chmelka and A. Pines, "Some Developments in NMR of Solids,"
>Science (Washington, DC), 246, 71 (1989).
>
>66. H. Saito and I. Ando, "High-Resolution Solid-State NMR Studies of
>Synthetic and Biological Macromolecules," Annu. Rep. NMR Spectrosc.,
>21, 209 (1989).
>
>67. J.F. Stebbins and I. Farnan, "NMR Spectroscopy in the Earth
>Sciences: Structure and Dynamics," Science (Washington, DC), 245, 257
>(1989).
>
>68. D.E. Woessner, "Characterization of Clay Minerals by Al-27 NMR
>Spectroscopy," Am. Mineral., 74, 203 (1989).
>
>69. G.B. Manelis, L.N. Erofeev, B.N. Provotorov, and A.K. Khitrin,
>Eds., "Pulsed NMR Study of Molecular Motion in Solids," Volume 14,
>Part 2, Harwood Academic, NY, 1989.
>
>70. J.-Ph. Ansermet, C.P. Slichter, and J.H. Sinfelt, "Solid-State NMR
>Techniques for the Study of Surface Phenomena," Prog. Nucl. Magn.
>Reson. Spectrosc., 22, 401 (1990).
>
>71. J. Klinowski and M.W. Anderson, "Solid-State NMR Studies of the
>Structure & Reactivity of Molecular Sieve Catalysts," Magn. Reson.
>Chem., 28, S68 (1990).
>
>72. A.J. Vila, C.M. Lagier, and A.C. Olivieri, "High-Resolution
>Solid-State NMR Study of Reversible 1,5-Proton Shifts in Organic
>Solids," Magn. Reson. Chem., 28, S29 (1990).
>
>73. A.E. Derome and S. Bowden, "Low-Temperature Solid-State NMR of
>Proteins," Chem. Rev., 91, 1307 (1991).
>
>74. C.A. Fyfe, Y. Feng, H. Grondey, G.T. Kokotailo, and H. Gies, "One-
>and Two-Dimensional High-Resolution Solid-State NMR Studies of Zeolite
>Lattice Structures," Chem. Rev., 91, 1525 (1991).
>
>75. R.K. Harris and P. Jackson, "High-Resolution Fluorine-19 Magnetic
>Resonance of Solids," Chem. Rev., 91, 1427 (1991).
>
>76. J. Klinowski, "Solid-State NMR Studies of Molecualr Sieve
>Catalysts," Chem. Rev., 91, 1459 (1991).
>
>77. V.M. Mastikhin, I.L. Mudrakovsky, and A.V. Nosov, "1H NMR Magic
>Angle Spinning Studies of Heterogeneous Catalysis," Prog. Nucl. Magn.
>Reson. Spectrosc., 23, 259 (1991).
>
>78. L.J. Mathias, Ed., "Solid State NMR of Polymers," Plenum Press,
>NY, 1991.
>
>79. H.W. Spiess, "Structure and Dynamics of Solid Polymers from 2D-
>and 3D-NMR," Chem. Rev., 91, 1321 (1991).
>
>80. D. Brinkmann, "NMR Studies of Superionic Conductors," Prog. Nucl.
>Magn. Reson. Spectrosc., 24, 527 (1992).
>
>81. N.J. Clayden, "Developments in Solid State NMR," Annu. Rep. NMR
>Spectrosc., 24, 1 (1992).
>
>82. D.G. Cory, "Solid State NMR Imaging," Annu. Rep. NMR Spectrosc.,
>24, 87 (1992).
>
>83. H. Eckert," Structural Characterization of Noncrystalline Solids &
>Glasses Using Solid State NMR," Prog. Nucl. Magn. Reson. Spectrosc.,
>24, 159 (1992).
>
>84. R.K. Harris and A.C. Olivieri, "Quadrupolar Effects Transferred to
>Spin-1/2 Magic-Angle Spinning Spectra of Solids," Prog. Nucl. Magn.
>Reson. Spectrosc., 24, 435 (1992).
>
>85. O.B. Lapina, V.M. Mastikhin, A.A. Shubin, V.N. Krasilnikov, and
>K.I. Zamaraev, "51V Solid State NMR Studies of Vanadia Based
>Catalysts," Prog. Nucl. Magn. Reson. Spectrosc., 24, 457 (1992).
>
>86. E. Wrenn Wooten, K.T. Mueller, and A. Pines, "New Angles in NMR
>Sample Spinning," Acc. Chem. Res., 25, 209 (1992).
>
>87. R.E. Botto and Y. Sanada, Eds., "Magnetic Resonance of
>Carbonaceous Solids," American Chemical Society, Washington, DC, 1993,
>Adv. Chem. Ser. No. 229.
>
>88. D. Freude and J. Haase, "Quadrupole Effects in Solid-State NMR,"
>NMR Basic Prin. Prog., 29, 1 (1993).
>
>89. R.K. Harris, "State of the Art for Solids," Chem. Brit., 29, 601
>(1993).
>
>90. A. Shoji, S. Ando, S. Kuroki, I. Ando, and G.A. Webb, "Structural
>Studies of Peptides and Polypeptides in the Solid State by Nitrogen-15
>NMR," Annu. Rep. NMR Spectrosc., 26, 55 (1993).
>
>91. J.S. Waugh, "NMR Spectroscopy in Solids: A Historical
>Perspective," Anal. Chem., 65, 725A (1993).
>
>92. F.D. Blum, "NMR Studies of Organic Thin Films," Annu. Rep. NMR
>Spectrosc., 28, 277 (1994).
>
>93. B. Bl=FCmich, Ed., "Solid-State NMR, 1: Methods," NMR Basic Prin.
>Prog., 30, articles therein (1994).
>
>94. B. Bl=FCmich, Ed., "Solid-State NMR, 2: Inorganic Matter," NMR Basic
>Prin. Prog., 31, articles therein (1994).
>
>95. B. Bl=FCmich, Ed., "Solid-State NMR, 3: Organic Matter," NMR Basic
>Prin. Prog., 32, articles therein (1994).
>
>96. B. Bl=FCmich, Ed., "Solid-State NMR, 4: Methods & Applications of
>Solid-State NMR," NMR Basic Prin. Prog., 33, articles therein (1994).
>
>97. T.A. Cross, "Structural Biology of Peptides and Proteins in
>Synthetic Membrane Environments by Solid-State NMR Spectroscopy,"
>Annu. Rep. NMR Spectrosc., 29, 123 (1994).
>
>98. S. Hayashi, "High-Resolution Solid-State NMR Studies on Ceramics,"
>Annu. Rep. NMR Spectrosc., 28, 29 (1994).
>
>99. H. Kawazoe, "Application of NMR Spectroscopy to the Science &
>Technology of Glasses & Ceramics," Annu. Rep. NMR Spectrosc., 28, 1
>(1994).
>
>100. H. Kurosu, S. Ando, H. Yoshimizu, and I. Ando, "NMR Studies of
>Higher-Order Structures of Solid Polymers," Annu. Rep. NMR Spectrosc.,
>28, 189 (1994).
>
>101. H. Pfeifer and H. Ernst, "NMR Studies of Zeolites," Annu. Rep.
>NMR Spectrosc., 28, 91 (1994).
>
>102. K. Schmidt-Rohr and H.W. Spiess, "Multidimensional Solid-State
>NMR of Polymers," Academic Press, NY, 1994.
>
>103. E.O. Stejskal and J.D. Memory, "High Resolution NMR in the Solid
>State: Fundamentals of CP/MAS," Oxford University Press, NY, 1994.
>
>104. E.R. Andrew and E. Szczesniak, "A Historical Account of NMR in
>the Solid State," Prog. Nucl. Magn. Reson. Spectrosc., 28, 11 (1995).
>
>105. P.J. Barrie, "NMR Applications to Porous Solids," Annu. Reports
>NMR Spectrosc., 30, 37 (1995).
>
>106. K.D.M. Harris and A.E. Aliev, "Solid Dynamics," Chem. Brit., 31,
>132 (1995).
>
>107. F.P. Miknis, "Applications of Solid-State NMR in Oil Shale
>Research," Annu. Reports NMR Spectrosc., 33, 207 (1997).
>
>108. C. Ye, S. Ding, and J. Zhou, "Progress in High-Resolution NMR in
>Solids," Annu. Reports NMR Spectrosc., 33, 37 (1997).
>
>109. N. Asakawa, T. Kameda, S. Kuroki, H. Kurosu, S. Ando, I. Ando,
>and A. Shoji, "Structural Studies of Hydrogen-Bonded Peptides and
>Polypeptides by Solid-State NMR," Annu. Reports NMR Spectrosc., 35, 55
>(1998).
>
>110. E. Brunner and U. Sternberg, "Solid-State NMR Investigations on
>the Nature of Hydrogen Bonds," Prog. Nucl. Magn. Reson. Spectrosc.,
>32, 21 (1998).
>
>111. R. Bruschweiler, "Dipolar Averaging in NMR Spectroscopy: from
>Polarization Transfer to Cross Relaxation," Prog. Nucl. Magn. Reson.
>Spectrosc., 32, 1 (1998).
>
>112. P. Colombet, "NMR Spectroscopy of Cement-Based Materials,"
>Springer-Verlag, NY, 1998.
>
>113. J. Grandjean, "NMR Studies of Interfacial Phenomena," Annu.
>Reports NMR Spectrosc., 35, 217 (1998).
>
>114. J.J. Fitzgerald, Ed., "Solid-State NMR Spectroscopy of Inorganic
>Materials," American Chemical Society, Washington, DC, 1999, ACS Symp.
>Ser. No. 717.
>
>115. A.M. Gil and C. Pascoal Neto, "Solid-State NMR Studies of Wood
>and Other Lignocellulosic Materials," Annu. Rep. NMR Spectrosc., 37,
>75 (1999).

Dr. Joseph Vaughn
Associate Director, NMR Facility
Chemistry Department
=46lorida State University
Tallahassee, FL 32306-4390
Phone 850-644-3334
=46ax 850-644-8281
email vaughn@pro.sb.fsu.edu