AMMRL: 13C CPMAS of flims

From: Kenneth Knott <kknott_at_vt.edu>
Date: Fri, 21 Oct 2016 15:49:34 -0400

I have a student who wishes to do some 13C CPMAS of polymer films.
Apparently they are not able to be crushed into a powder as would be idea
for as CPMAS rotor. What technique is preferred for this analysis?

I'm seen some references to packing the film into the rotor and filling the
dead space with KBr.

Thanks!

-- 
Ken Knott
Department of Chemistry
Analytical Services
Virginia Tech
(540)267-6502 (Cell)
(540)231-0885 (Office)

Received on Fri Oct 21 2016 - 09:49:30 MST