Hi AMMRLers,
I would like to thank Kris Kolonko, Dan Wherritt, Dean Olson, Stefan
Berger and Lingyang Zhu for sending papers about the rapid injection
systems used. The abbreviated citations to the articles are below:
(Chem. Ber. 1993, 126, 2397 -2401)
(J. Org. Chem. 1984,49,4465-4470)
(J. AM. CHEM. SOC. 2003, 125, 12484-12492)
(J. Org. Chem. 2010, 75, 5558–5572)
(J. AM. CHEM. SOC. 2007, 129, 3492-3493) - details in SI
https://search.library.wisc.edu/catalog/9910086804802121 - introduction
chapter
I would also like to post an interesting product that Charlie Fry found
from New Era that advertises a reaction chamber inside the tube using a
tube within a tube design for loading the two components. It requires
the ejection of the sample from the probe to mix the reagents but does
not require physical removal from the bore. This may be a more
affordable alternative solution for people not wanting to expose a cold
sample to air but do not need the speed of a rapid injection system.
http://newera-spectro.com/sample-reaction-system
Thank you for your help!
Take care,
Paul
--
Dr. Paul White
Institute for Molecules and Materials
Radboud University Nijmegen
+31 (0)24 365 2959
P.White_at_science.ru.nl
Received on Tue Oct 18 2016 - 05:25:50 MST