Re: AMMRL:perfect-CLIP-HSQC

From: Ron Crouch <roncrouch1_at_mac.com>
Date: Mon, 21 Nov 2016 12:24:45 -0600

Hi Alan,

It should be in the Spinsights user library! I put it there right about
at the time we all got chopped!!

It is coded "pure chempack" meaning it needs Chempack or std VnmrJ 4.2
or beyond to work. I added a new module for that one which has a
composite chirp refocusing 13C pulse.


It has an option for bipolar 13C decoupling to allow silly ~3 sec F2
acquisition time which I'd say to not bother with. For RDC's it is much
better to measure J in F1. I have an experiment for that as well which
needs testing. (no Varianese NMR access for me these days).


Pulse me at roncrouch1_at_mac.com if there is a problem.


Clear skies,

Ron


On 11/21/2016 7:11 AM, KENWRIGHT, ALAN M. wrote:
> Hi All,
>
> I am short of time and in a rush (what’s new?) Does anyone have a version of the perfect-CLIP-HSQC sequence (Castanar et al, Magn. Reson. Chem. 2015, 53, 115–119) coded for a Vagilent that they would be willing to share?
>
> Kind regards,
>
> Alan
>
> Alan Kenwright
> Reader in Spectroscopy & NMR Service Manager
> Durham University Chemistry Department
>
Received on Mon Nov 21 2016 - 08:24:52 MST

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