Dear All
Does anyone have any guidelines / rules-of-thumb for setting mixing times in metal-1H HOESY experiments? I'm particularly interested in 195Pt-1H but so far I've had no success. There's plenty of literature that refers to the use of HOESY experiments but relatively little on the selection of appropriate mixing times, or the reasons why a particular mixing time has been used (I've ordered Kover and Batta's papers from our library service but that usually takes a while).
Any advice will be appreciated and I'll post a follow up if anyone else is interested in the topic.
Thank-you,
Craig.
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Craig Grimmer
UNPCHEMNMR
School of Chemistry
University of KwaZulu-Natal
Private Bag X01
Pietermaritzburg
3209
South Africa
Tel: +27-33-2605326/5984
Fax: +27-33-2605009
Email: grimmerc_at_ukzn.ac.za
URL: http://chemweb.unp.ac.za/NMRlab/
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Received on Sat Mar 19 2011 - 00:55:05 MST