Dear Colleagues,
Thank you very much who answered my question about 2J and 3J Si-H
coupling. Some references about Si-H coupling are listed below.
1) "NMR and the Periodic Table" edited by Harris and Mann, Academic
press 1978, page 329 : 2J(H,Si) = 1 to 13 Hz and 3J(H,Si) = 1 to 8 Hz
2) Schraml J., Bellama J.M.: 29Si nuclear magnetic resonance.
Determination of Organic Structures by Physical Methods 6, 203 (1976).
3) Schraml J.: 29Si NMR spectroscopy of trimethylsilyl tags. Progress
NMR Spectroscopy 22, 289 (1990).
4) Schraml J.: 29Si NMR Experiments in solutions of organosilicon
compounds.In "The chemistry of organic silicon compounds, Vol.3
(Rappoprt Z., and Apeloig Y, Eds) Wiley, 2001.
5) There is a good book which has a chapter on Silicon 1.Multinuclear
NMR edited by Joan Mason 1987 Plenum Publishing Corporation ISBN
0-306-42153-4
6) P.Diehl, E.Fluck and R.Kostfeld EDS. NMR Basic Principles and
Progress, Springer, Berlin. Vol 1, 1969 to vol 17 1981 . Oxygen 17 and
Silicone 29" Vol 18 , (1981)
Best regards,
Miriam
Received on Thu Mar 07 2002 - 09:10:47 MST