Re: thallium NMR

From: lew cary <lcary_at_chem.unr.edu>
Date: Wed, 15 Mar 2000 09:52:28 -0800 (PST)

In the last year we have done Tl205. We used Nitrate to locate the
resonance easily in a 5mm probe. However, the metal complexs we wanted to
look at were a lot of pain. I set the U+ to 1000 scans and searched 100KHz
at a time. Even under these circumstances AV mode was the best way to see
the signal the first time. It turned out that I should have used an LB of
100 HZ!! I had no clue that Tl would be so broad. More info an the ENC
poster W/Th PD 182.
        Cheers, Lew
Received on Wed Mar 15 2000 - 12:26:49 MST

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