Hi,
I've found that with some of the 15N relaxation pulse sequences, I have uneven phase correction across the spectrum. A regular HSQC phases just fine, but the spectra from a T! experiment, does not. (hsqct1etf3gpsi3d) I've used a d1 of 4s for the t1 experiment.
Any suggestions would be greatly appreciated.
Tara
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Dr. Tara Sprules
QANUC
Quebec/Eastern Canada High Field NMR Facility
www.nmrlab.mcgill.ca
phone: (514) 398-1721
fax: (514) 398-8254
3420 University St., Rm 023
McGill University
Montreal, QC, H3A 2A7
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Received on Sun Jun 21 2020 - 07:42:50 MST