AMMRL: Running VT NMR above solvent's bp

From: Dobrowolski, Piotr <Piotr.Dobrowolski_at_ttu.edu>
Date: Thu, 6 Jun 2019 21:03:42 +0000

Hello Everyone,
One of the users of our 400 MHz JEOL ECS spectrometers would like to run her experiment for more than 10 h (reaction monitoring) in THF at 70 deg. C. Do you have any experience with running such experiments? If yes, what high or medium-pressure 5 mm tubes can you recommend. So far we've been thinking about Wilmad or NewEra products.
Thank you,
Piotr


Piotr Dobrowolski, Ph.D.
Sr. Research Associate - NMR Facility Manager

Department of Chemistry & Biochemistry
Texas Tech University
Chemistry Bldg Room 051
1204 Boston Ave, Lubbock, TX 79409,
Telephone: (806) 834-7706
Email: piotr.dobrowolski_at_ttu.edu<mailto:piotr.dobrowolski_at_ttu.edu>

https://www.depts.ttu.edu/chemistry/Facilities/nmrlab/<https://na01.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.depts.ttu.edu%2Fchemistry%2FFacilities%2Fnmrlab%2F&data=02%7C01%7Cpiotr.dobrowolski%40ttu.edu%7C531bbb6b34c542967f5e08d627c094e1%7C178a51bf8b2049ffb65556245d5c173c%7C0%7C0%7C636740105947076991&sdata=t1fhIh9uVlA6ytqTv%2F8K4tgFRCwSFBDfw3lGKlaYMdA%3D&reserved=0>
Received on Thu Jun 06 2019 - 11:04:11 MST

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