Dear AMMRLers,
For the rare cases that certain project requires high temperature NMR experiment above the solvent boiling point, for example, 40c above boiling point of DCM, will you allow the users to run it? If the NMR tube is sealed, it could increase the boiling point to an extended degree, which we have done on our 200M NMR before successfully with other solvent. However, now similar work needs to be done on the 500M NMR (which is our major instrument for all organic users) for extended hours, I am a little concerned and would like to hear advice/suggestions/tricks on this issue, thanks.
Fei
Fei Yang, Ph.D
Instrumentation Specialist
Department of Chemistry & Biochemistry
Miami University, Oxford, OH
Rm 76B Hughes
701E High Street
513-529-3163
Received on Fri Jul 06 2012 - 09:44:55 MST