Happy New Year everyone.
Has anyone had any experience with the N15 T2 exchange experiment (gNcpmgex_NH) in BioPack? We can't seem to get it to work or even see any signal in the first increment, even when the number of CPMG cycles is very low. Other BioPack sequences seem to work fine, suggesting that the probe calibration file is fine. Checking on the SPINSIGHTS site, it appears that at least one other person has had trouble with this experiment (in both VJ 3.2 and 4), but there was no real fix that I could see.
This is an INOVA600 running VnmrJ 3.2A.
Thanks!
Kirk
Kirk Marat, Ph. D. NMR Facility Manager
Dept. of Chemistry, University of Manitoba
Winnipeg, Manitoba
R3T 2N2, Canada
Ph: (204) 474-6259 FAX: (204) 474-7608
Received on Fri Jan 03 2014 - 11:25:40 MST