NMR lineshape problem

From: Zhang, Weixing <Weixing.Zhang_at_stjude.org>
Date: Wed, 23 Jan 2002 13:11:09 -0600

Hello everybody:

I recently got a nonspin lineshape spectrum with extra peaks.
If I set the main CHCl3 peak at 0 Hz, I saw extra small peaks
at -111 Hz, -57 Hz, 57 Hz, and 111 Hz. Their intensity is about half
of the C13 satellite peaks. What might be the problem?

I closely looked at the normal lineshape spectrum. The two
C13 satellite peaks are located at -109 Hz and 106 Hz.
Does anybody know why they are not symmetrical (-107.5, 107.5 Hz).

Thanks,

Weixing Zhang, Ph.D.
Department of Structural Biology
St. Jude Children's Research Hospital
Voice: (901)495-3169
FAX: (901)495-3032
Received on Wed Jan 23 2002 - 13:31:00 MST

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