AMMRL: New ASTM Effort to Develop NMR Standards

Jane Strouse (strousej@chem.ucla.edu)
Thu, 7 Feb 2008 17:37:13 -0800


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Dear AMMRL'ers,

 

     I am forwarding the message below on behalf of Gary Kramer of NIST
who is looking for volunteers to help formulate new NIST standards for
NMR.  Please respond to him directly if you are interested.  His contact
information is give at the bottom of his message.

 

Jane

 

----------------------------------------------------------------------

Dr. Jane Strouse

Director, UCLA Molecular Instrumentation Center

1410 Molecular Sciences Building

Los Angeles, CA 90095-1569

(310)-825-9841 - voice

(310)-825-2280 - fax

strousej@chem.ucla.edu

http://www.mic.ucla.edu

----------------------------------------------------------------------

 

 

Hi folks,

 

As I have mentioned to several of you on the phone (and I apologize to
those 

that I have not been able to reach), I am attempting to rekindle an ASTM


effort to develop standards (both artifact and procedural) for NMR 

spectroscopy.  I chair the ASTM Subcommittee E13.15 on Analytical Data.
When 

the E13 Committee was reorganized a few years back, the inactive NMR 

subcommittee was disbanded, and their sole standard, E386-90 "Standard 

Practice for Data Presentation Relating to Nuclear Magnetic Resonance
(NMR) 

Spectroscopy," was moved into E13.15 for two reasons--the standard had
the 

word "data" in its title, and the E13 chairman knew that I could spell
NMR.

 

The E386 standard was developed in the mid-1970s and was last revised in
1990.  

A lot has happened to the state of the art and practice of NMR since
then.  

Furthermore, when we bought a spectrometer a few years ago, I was
pleasantly 

surprised to see that the vendors' specs appeared to be generated using 

similar samples, indicating the existence of some de facto agreements
toward 

standards in the community.  Accordingly, it seems to me that the time
may be 

ripe to revive an effort to develop NMR standards at ASTM.  Judging from
my 

phone conversations, a lot of you agree.

 

I envision that the process to develop new NMR standards could primarily
be 

conducted via Internet-assisted conference calls (aka Virtual Meetings
or 

VMs).  We have been using VMs very effectively for other E13.15
activities 

over the past three years, and ASTM has a good system in place to
facilitate 

VMs.  However, with PittCon coming up very soon, I have secured a 1-hour
time 

slot in the ASTM meeting room that those of us who are attending PittCon
can 

use to discuss this project face-to-face.  This meeting will be at 10:00
AM, 

Monday, March 3 in Room MR-05, which I'm told is on the second level in
the 

Conference Center.  If you are not personally attending PittCon, feel
free to 

deputize someone from your company who is or to pass this along to other


interested parties/stakeholders.  If you know of others that I should 

contacted about this, please let me know.  I look forward to working
with all 

of you on this and, as always, am eager to hear to what you have to say
on 

this subject.

 

Cheers,

Gary Kramer

Research Chemist

 

NIST

Biochemical Science Division

Stop 8310

Gaithersburg, MD  20899

301-975-4132

gary.kramer@nist.gov

 

 

 


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Dear AMMRL’ers,

 

     I am forwarding the message = below on behalf of Gary Kramer of NIST who is looking for volunteers to help = formulate new NIST standards for NMR.  Please respond to him directly if you = are interested.  His contact information is give at the bottom of his = message.

 

Jane

 

------------------------------------------------------= ----------------

Dr. Jane Strouse

Director, UCLA Molecular Instrumentation Center

1410 Molecular Sciences Building

Los Angeles, CA 90095-1569

=

(310)-825-9841 - voice

(310)-825-2280 - fax

strousej@chem.ucla.edu<= /font>

http://www.mic.ucla.edu

------------------------------------------------------= ----------------

 

 

Hi = folks,

 

As I have mentioned = to several of you on the phone (and I apologize to those

that I have not = been able to reach), I am attempting to rekindle an ASTM

effort to develop = standards (both artifact and procedural) for NMR

spectroscopy.  = I chair the ASTM Subcommittee E13.15 on Analytical Data.  When =

the E13 Committee = was reorganized a few years back, the inactive NMR

subcommittee was = disbanded, and their sole standard, E386-90 "Standard

Practice for Data Presentation Relating to Nuclear Magnetic Resonance (NMR) =

Spectroscopy," = was moved into E13.15 for two reasons--the standard had the =

word = "data" in its title, and the E13 chairman knew that I could spell = NMR.

 

The E386 standard = was developed in the mid-1970s and was last revised in 1990.  =

A lot has happened = to the state of the art and practice of NMR since then.  =

Furthermore, when = we bought a spectrometer a few years ago, I was pleasantly

surprised to see = that the vendors' specs appeared to be generated using

similar samples, = indicating the existence of some de facto agreements toward

standards in the community.  Accordingly, it seems to me that the time may be =

ripe to revive an = effort to develop NMR standards at ASTM.  Judging from my

phone = conversations, a lot of you agree.

 

I envision that the = process to develop new NMR standards could primarily be

conducted via Internet-assisted conference calls (aka Virtual Meetings or =

VMs).  We have = been using VMs very effectively for other E13.15 activities =

over the past three = years, and ASTM has a good system in place to facilitate

VMs.  However, = with PittCon coming up very soon, I have secured a 1-hour time

slot in the ASTM = meeting room that those of us who are attending PittCon can

use to discuss this = project face-to-face.  This meeting will be at 10:00 AM,

Monday, March 3 in = Room MR-05, which I'm told is on the second level in the

Conference Center.  If you are = not personally attending PittCon, feel free to

deputize someone = from your company who is or to pass this along to other

interested parties/stakeholders.  If you know of others that I should =

contacted about = this, please let me know.  I look forward to working with all

of you on this and, = as always, am eager to hear to what you have to say on

this = subject.

 

Cheers,

Gary = Kramer

Research = Chemist

 

NIST

Biochemical Science = Division

Stop = 8310

Gaithersburg, MD  = 20899

301-975-4132

gary.kramer@nist.gov

 

 

 

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