AMMRL: air sensitive sample for CP/MAS

From: Charles G. Fry <fry_at_chem.wisc.edu>
Date: Wed, 07 Dec 2011 01:11:19 -0600

Hi all,

I've recently been having fun re-learning some solid-state NMR. But
have a request to run a sample that is air sensitive. We used to go
through serious contortions back when I was young(er?) handling such
samples in MAS rotors. But it's been a long time since I last did
anything similar. It would really help to hear what new tricks might
have come up to do this better. If you work with similar samples, we'd
really appreciate hearing how you handle the samples. We are using a
Bruker CP/MAS probe with 4mm rotors (single cap at top). I'll be happy
to summarize the responses

Charlie

-- 
~~~~~~~~~~~~~~~~~~~~~~~
Charles G. Fry, Ph.D.              Tel:  (608)262-3182
Director, MR Facility              Fax:  (608)262-0381
Chem. Dept., 1101 University Ave, Univ. Wisconin-Madison
Madison, WI  53706  USA        email:  fry_at_chem.wisc.edu
Received on Tue Dec 06 2011 - 21:11:24 MST

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