Re: AMMRL: rolling basline on 31P solid state NMR spectra

From: David Rice <daverice_at_stanford.edu>
Date: Tue, 18 Aug 2015 11:53:08 -0700

Hi Megan

I am happy to help you if you want to email me privately -
daverice_at_stanford.edu. I was formerly the Solids applications
person for Varian and Agilent. The exact procedure depends on the
sequence -- but you will need to set the parameters
rof2 and alfa (or rd and ad) correctly on the INOVA. Once I know your
sequence and parameters I can figure out what is wrong.

Dave

On 8/18/2015 7:38 AM, Kirk, Megan (MM) wrote:
>
> Hello everyone,
>
> How does one prevent a rolling baseline in solid state 31P NMR on a
> narrow bore Varian 600 MHz, Unity Inova? I know I can remove it
> afterwards by integration and then using dc and bc. How do I prevent
> it in the first place?
>
> Thanks for your help,
>
> Megan Kirk
>
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Received on Tue Aug 18 2015 - 08:53:16 MST

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