Dear Members,
I have acquired some 2H NMR spectra on a BRUKER AVANCE DRX500 with a BBI 5mm
probe through the X-BB channel (I removed the 2H-stop filter and the 2H
cable).
I used the zg and zgpg pulse-programs but I 'm not able to phase the spectra
only with phases about 500-700 degrees (ph0 and ph1).
I have two signals (one big from CDCl3 and one from the labeled molecule :
the intensity and phase of the last one depend on number of scans).
Could you explain to me this problem of phase?
Thank you for your help.
_______________________________________________________
Guillaume CHAPDELAINE
RHONE-POULENC INDUSTRIALISATION
CRIT Décines
ANA/STR/RMN
24, Avenue Jean Jaurès
69153 DECINES CHARPIEU Cedex
FRANCE
Tél. : (33) (0)4 72 93 59 70
Fax : (33) (0)4 72 93 54 43
Cour. : guillaume.chapdelaine_at_crit.rhone-poulenc.com
Received on Thu Aug 30 2001 - 09:17:30 MST