Here are some resources that I have consulted:
Gorenstein, David G. Phosphorus-31 NMR : principles and
applications. Orlando, Fla. : Academic Press, 1984
Burt, C. T. Phosphorus NMR in Biology; CRC Press: Boca Raton, FL 1987.
On Wednesday, March 31, 2004, at 09:23 AM, Robert Wiseman wrote:
>
> AMMRLers-
>
> We have been working with a small cell bioreactor doing phosphorus NMR
> to detect chemical potential changes arising from glucose challenges.
> We have done some extracts and found many resonances in the sugar
> phosphate regions that do not correspond with what we expected. These
> are likely glycolytic intermediates I suspect. I have been looking
> for a good reference (book or manuscript) that describes the chemical
> shift positions of biologically active phosphorus compounds at pH
> ranges from 6.9-7.1. I recall a book in the mid to late 80's that
> had a chapter dedicated to this that included every biologically
> active phosphate compound, its chemical shift and the pKa if it was an
> ionizable compound. I do not recall the reference and have been
> unable to locate the book, does anyone recall this chapter?
>
> Any recommendation for a decent paper would also be quite helpful. I
> have found references for phosphorus compounds in general, even some
> web sources, but specific glycolytic intermediates were not listed.
> Thanks
>
>
>
> Robert W. Wiseman, Ph.D.
> Associate Professor of Physiology and Radiology
>
> Shipping and Mailing Address:
> Michigan State University
> Department of Physiology
> 2201 Biomedical and Physical Sciences Building
> East Lansing, MI 48824
>
> email: rwiseman_at_msu.edu
> alternative email (for files larger than 500 KByte): rww_at_rad.msu.edu
>
> office 3198 BPS Building
> 517-355-6475 (x-1151)
> laboratory 3110 BPS Building
> 517-355-6475 (x-1342)
>
>
Judith C. Amburgey-Peters
Associate Professor of Chemistry
College of Wooster
Department of Chemistry
943 College Mall
Wooster, OH 44691
330-263-2014 voice
330-263-2386 fax
Progress involves risk. You cannot steal second and keep your foot on
first. (Unknown)
Received on Thu Apr 01 2004 - 17:44:43 MST