AMMRL: Diffusion questions

Neal J Stolowich (stolowich@louisville.edu)
Thu, 14 Feb 2008 16:35:18 -0500 

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Greetings!

I'm in the process of trying some diffusion experiments for the first =
time, and have some questions regarding their implementation on a Varian =
INOVA spectrometer, running 6.1B with the appropriate diffusion =
"package" loaded from CD and with "diffusion" downloaded and extracted =
out of the userlib. I believe I understand the general gist of the =
experimental setup scheme from the VNMR liquids guide, but wanted to =
check on a few of the parameters.  Obviously, the first step in gradient =
calibration of a d2o sample. If you've run these before and could answer =
a few questions, a reply would be appreciated.

Thanks!

Neal

Neal J Stolowich, PhD
NMR Facilities Manager
Department of Chemistry
University of Louisville
Louisville, KY 40209
Phone: (502) 852-7894=20
Fax: (502) 852-8149
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Greetings!


 


I'm in the process of trying some =
diffusion=20
experiments for the first time, and have some questions regarding their=20
implementation on a Varian INOVA spectrometer, running 6.1B with the =
appropriate=20
diffusion "package" loaded from CD and with "diffusion" downloaded =
and=20
extracted out of the userlib. I believe =
I understand the=20
general gist of the experimental setup scheme from the VNMR liquids =
guide, but=20
wanted to check on a few of the parameters.  Obviously, the first =
step in=20
gradient calibration of a d2o sample. If you've run these before and =
could=20
answer a few questions, a reply would be =
appreciated.


 


Thanks!


 


Neal


 


Neal J Stolowich, PhD
NMR Facilities =

Manager
Department of Chemistry
University of =
Louisville
Louisville, KY=20
40209
Phone: (502) 852-7894 
Fax: (502)=20
852-8149


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